Different Analytical Procedures for the Study of Organic Residues in Archeological Ceramic Samples with the Use of Gas Chromatography-mass Spectrometry

Different Analytical Procedures for the Study of Organic Residues in Archeological Ceramic Samples with the Use of Gas Chromatography-mass Spectrometry
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DOI:
10.1080/10408347.2015.1008130
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发表时间:
2016-01
影响因子:
5
通讯作者:
J. Kałużna-Czaplińska;Angelina Rosiak;M. Kwapinska;W. Kwapinski
J. Kałużna-Czaplińska;Angelina Rosiak;M. Kwapinska;W. Kwapinski
中科院分区:
化学2区
文献类型:
--
作者:
J. Kałużna-Czaplińska;Angelina Rosiak;M. Kwapinska;W. Kwapinski

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摘要陶器中有机残留物的组成分析是历史学家和考古学家的重要信息来源。材料的化学特征提供了有关饮食、习惯、技术和血管原始用途的信息。本文介绍了考古材料的分析研究中存在的问题,特别强调了有机残留物。介绍了目前考古陶瓷中不同有机化合物的测定方法。重点介绍了考古陶瓷样品在气相色谱-质谱分析前的分析方法。讨论了不同提取方法的优缺点和适当的质量保证/质量控制程序的应用。
ABSTRACT The analysis of the composition of organic residues present in pottery is an important source of information for historians and archeologists. Chemical characterization of the materials provides information on diets, habits, technologies, and original use of the vessels. This review presents the problem of analytical studies of archeological materials with a special emphasis on organic residues. Current methods used in the determination of different organic compounds in archeological ceramics are presented. Particular attention is paid to the procedures of analysis of archeological ceramic samples used before gas chromatography-mass spectrometry. Advantages and disadvantages of different extraction methods and application of proper quality assurance/quality control procedures are discussed.