Silicon tetrafluoride : Preparation and reduction with lithium aluminium hydride

Silicon tetrafluoride : Preparation and reduction with lithium aluminium hydride
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DOI:
10.1016/s0022-1139(00)82975-9
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发表时间:
1979-10
影响因子:
1.9
通讯作者:
D. Padma;B. S. Suresh;A. Vasudevamurthy
D. Padma;B. S. Suresh;A. Vasudevamurthy
中科院分区:
化学4区
文献类型:
--
作者:
D. Padma;B. S. Suresh;A. Vasudevamurthy

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Pure silicon tetrafluoride can be prepared in 66% yield from silicon tetrachloride by refluxing with lead fluoride in acetonitrile. The gas can be reduced to pure silane by lithium aluminum hydride in diethyl ether.