A robust, sensitive, and versatile HMBC experiment for rapid structure elucidation by NMR: IMPACT-HMBC
A robust, sensitive, and versatile HMBC experiment for rapid structure elucidation by NMR: IMPACT-HMBC
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DOI：
10.1039/c000964d
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发表时间：
2010-01-01
影响因子：
4.9
通讯作者：
Furrer, Julien
中科院分区：
文献类型：
--
作者：
Furrer, Julien
描述了一个强大的、通用的、易于优化的HMBC实验，用于复杂的有机结构解析，该实验已在醋酸胆固醇、环孢素和异丙基甘油上进行了实验测试。所提出的实验，IMPACT-HMBC（改进和加速的恒定时间异核多键相关），结合了灵敏度，实验设置简单，可以在短的恢复时间内记录。
A robust, versatile and easy to optimize HMBC experiment for complex organic structure elucidation which has been experimentally tested on cholesteryl acetate, cyclosporine and isopropylidene glycerol is described. The proposed experiment, IMPACT-HMBC (improved and accelerated constant-time heteronuclear multiple-bond correlation), combines sensitivity, easy experimental setup and can be recorded with short recovery times.