High-quality Fe(001) single crystal films on MgO(001) substrates for electron spectroscopies

High-quality Fe(001) single crystal films on MgO(001) substrates for electron spectroscopies
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用于电子光谱的 MgO(001) 基底上的高质量 Fe(001) 单晶薄膜

DOI:
10.1116/1.581340
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发表时间:
1998
期刊:
Journal of Vacuum Science and Technology
影响因子:
--
通讯作者:
F. Ciccacci
F. Ciccacci
中科院分区:
--
文献类型:
--
作者:
R. Bertacco;S. Rossi;F. Ciccacci

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通过在 MgO(001) 衬底上外延生长,在超高真空中制备了 Fe 薄膜。自旋分辨逆光电发射测量表明,未退火的覆盖层显示出比相应的本体系统更低的光谱质量。低能电子衍射和 X 射线光电子发射表明,退火会促进氧表面偏析,即使在数百埃厚的薄膜中也能产生 c(2×2) 重构。研究发现,相对较厚的薄膜(>1000 A)经过高温退火(~600 ℃)后可以获得表面洁净、有序的高质量Fe(001)单晶薄膜。
Fe films have been prepared in ultrahigh vacuum by epitaxial growth on MgO(001) substrates. Spin-resolved inverse photoemission measurements indicate that nonannealed overlayers display lower spectroscopic quality than the corresponding bulk system. Low energy electron diffraction and x-ray photoemission reveal that annealing promotes oxygen surface segregation giving rise to a c(2×2) reconstruction even in several hundred A thick films. It is found that high-quality Fe(001) single crystal films with clean and well ordered surfaces can be obtained after high temperature annealing (∼600 °C) of relatively thick films (>1000 A).