Evaluation of shear bond strength between PEEK and resin-based luting material
Evaluation of shear bond strength between PEEK and resin-based luting material
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DOI：
10.1016/j.job.2017.09.003
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发表时间：
2017-11-01
影响因子：
2.4
通讯作者：
Tsuga, Kazuhiro
中科院分区：
文献类型：
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作者：
Tsuka, Hiroki;Morita, Koji;Tsuga, Kazuhiro
目的：本研究的目的是评估聚醚醚酮（PEEK）与树脂基粘合材料的粘合强度。方法：将 80 个 PEEK 样品随机分为两组（n = 40/组）：未处理和喷砂。 40 个牙科金银钯合金样本（PALLAZ12-n；Yama-moto Precious Metal Co., Ltd.，大阪，日本）、氧化锆（Aadva Zirconia；GC，东京，日本）和混合复合树脂（CERASMART；GC，东京，日本）均用作 PEEK 的对照材料。每个组根据不同的树脂基粘合材料分为四个亚组 (n = 10)：Panavia (R) V5（Kuraray Medical，日本东京）、ReIyX (TM) Ultimate Resin Cement（3M ESPE，圣保罗，明尼苏达州，美国）、G-CEM Link Force（GC，日本东京）和 Super-Bond C&B（Sun Medical，西贺，日本）。将树脂基粘合材料粘合到样本上。所有标本均在37℃的蒸馏水中保存24小时。通过剪切测试测量粘合强度，并通过立体显微镜评估失效模式。经过各种预处理后，通过扫描电子显微镜观察表面。结果：与对照组相比，PEEK 组的大多数样品的剪切粘合强度显着较低（p < 0.05）。在PEEK组中，最常见的失效模式是材料与树脂基粘合材料之间的粘合失效。结论：本研究发现PEEK与树脂基粘合材料之间的粘合强度不足以满足PEEK的临床使用。 (C) 2017 年日本口腔生物学协会。由 Elsevier B.V. 出版。保留所有权利。
Objectives: The purpose of this study was to evaluate the bond strength of polyetheretherketone (PEEK) to resin-based luting material.Methods: Eighty PEEK specimens were randomly divided into two groups (n = 40/group): no treatment and sandblasting. Each of the 40 specimens of dental gold-silver-palladium alloy (PALLAZ12-n; Yama-moto Precious Metal Co., Ltd., Osaka, Japan), zirconia (Aadva Zirconia; GC, Tokyo, Japan), and hybrid composite resin (CERASMART; GC, Tokyo, Japan) was used as a control material for PEEK. Each group was divided into four subgroups (n = 10) for the different resin-based luting materials: Panavia (R) V5 (Kuraray Medical, Tokyo, Japan), ReIyX (TM) Ultimate Resin Cement (3M ESPE, St Paul, MN, USA), G-CEM Link Force (GC, Tokyo, Japan), and Super-Bond C&B (Sun Medical, Siga, Japan). The resin-based luting materials were bonded onto the specimens. All specimens were stored in distilled water at 37 degrees C for 24 h. Bond strength was measured with a shear test, and failure modes were assessed by stereomicroscopy. The surfaces were observed by scanning electron microscopy after the various pretreatments.Results: Compared with the control group, the PEEK group showed a significantly lower (p < 0.05) shear bond strength for most of the specimens. Among PEEK groups, the most frequent failure mode was adhesive failure between the material and the resin-based luting material.Conclusions: This study found that the bond strength between PEEK and resin-based luting materials was not adequate for clinical use of PEEK. (C) 2017 Japanese Association for Oral Biology. Published by Elsevier B.V. All rights reserved.