Compact low power infrared tube furnace for in situ X-ray powder diffraction
Compact low power infrared tube furnace for in situ X-ray powder diffraction
复制标题
DOI：
10.1063/1.4973561
复制
发表时间：
2017-01-01
影响因子：
1.6
通讯作者：
Gurlo, A.
中科院分区：
文献类型：
--
作者：
Doran, A.;Schlicker, L.;Gurlo, A.
我们描述了一个紧凑的，低功率的，红外加热的管式炉在原位粉末X射线衍射实验的发展和实施。我们基于碳化硅（SiC）的熔炉设计在精度控制和升温速率方面表现出出色的热性能，同时易于使用，抗滥用，并且由于其尺寸小，功耗低，对周围设备的影响最小。超过1100摄氏度的空气温度可以控制在优于1%的精度，温度上升速率高达100摄氏度/秒。完整的“附加”装置，减去电源，适合在一个圆柱形体积约15厘米长，直径6厘米，并居住在接近1厘米，从我们的实验同步加速器终端站的其他敏感组件没有不利影响。出版社：AIP Publishing
We describe the development and implementation of a compact, low power, infrared heated tube furnace for in situ powder X-ray diffraction experiments. Our silicon carbide (SiC) based furnace design exhibits outstanding thermal performance in terms of accuracy control and temperature ramping rates while simultaneously being easy to use, robust to abuse and, due to its small size and low power, producing minimal impact on surrounding equipment. Temperatures in air in excess of 1100 degrees C can be controlled at an accuracy of better than 1%, with temperature ramping rates up to 100 degrees C/s. The complete "add-in" device, minus power supply, fits in a cylindrical volume approximately 15 cm long and 6 cm in diameter and resides as close as 1 cm from other sensitive components of our experimental synchrotron endstation without adverse effects. Published by AIP Publishing.