An improved process for the synthesis of DMTMM-based coupling reagents
An improved process for the synthesis of DMTMM-based coupling reagents
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DOI：
10.1016/j.tetlet.2008.12.047
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发表时间：
2009-02-25
影响因子：
1.8
通讯作者：
Raw, Steven A.
中科院分区：
文献类型：
--
作者：
Raw, Steven A.
开发了一种简单、稳健和高产率的制备4-（4，6-二甲氧基-1，3，5-三嗪-2-基）-4-甲基吗啉四氟硼酸盐（DMTMM BF 4）和六氟磷酸盐（DMTMM PF 6）的方法，该方法避免了使用昂贵或不常见的试剂。(C)2008爱思唯尔有限公司保留所有权利。
A simple, robust and high-yielding process for the preparation of 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium tetrafluoroborate (DMTMM BF4) and hexafluorophosphate (DMTMM PF6) has been developed, which avoids the use of expensive or unusual reagents. (C) 2008 Elsevier Ltd. All rights reserved.