Morphology-controlling synthesis of ZnS through a hydrothermal/solvthermal method
Morphology-controlling synthesis of ZnS through a hydrothermal/solvthermal method
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DOI：
10.1016/j.ceramint.2011.10.013
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发表时间：
2012-04
影响因子：
5.2
通讯作者：
Ling Wang;J. Dai;Xizhong Liu;Zhibin Zhu;Xiang Huang;Pingwei Wu
中科院分区：
文献类型：
--
作者：
Ling Wang;J. Dai;Xizhong Liu;Zhibin Zhu;Xiang Huang;Pingwei Wu
以Zn（CH3COO）2·2H2O和SC（NH2）2为原料，在不同的混合溶剂中，通过改变表面活性剂（C12H25SO3Na）的浓度，采用溶剂热法合成了不同形貌的ZnS。采用X射线衍射（XRD）、扫描电子显微镜（SEM）和能谱分析（EDAX）对样品进行了表征。结果表明，所制备的ZnS具有不同的形貌，如层状ZnS、光滑微球、粗糙微球、片状ZnS等，但迄今为止，还没有用溶剂热法合成过层状ZnS。
Different morphologies of ZnS have been synthesized by a solvothermal process, through the reaction of Zn(CH3COO)2·2H2O and SC(NH2)2in different mixed solvents, changing the density of the surfactant (C12H25SO3Na). The samples were characterized by the X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy-dispersive X-ray analysis (EDAX) techniques. The results show that the as-prepared ZnS have different morphologies, such as lamellar ZnS, smooth microspheres, roughen microspheres, plate-like ZnS and so on. So far, to our knowledge, lamellar ZnS have not been synthesized by solvothermal route before.