Microwave-assisted deep eutectic-solvothermal preparation of iron oxide nanoparticles for photoelectrochemical solar water splitting
Microwave-assisted deep eutectic-solvothermal preparation of iron oxide nanoparticles for photoelectrochemical solar water splitting
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DOI：
10.1039/c7ta02078c
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发表时间：
2017-08-21
影响因子：
11.9
通讯作者：
Edler, Karen J.
中科院分区：
文献类型：
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作者：
Hammond, Oliver S.;Eslava, Salvador;Edler, Karen J.
在这里，我们提出了一种新的微波溶剂热法制备氧化铁纳米结构使用深共晶溶剂作为一个更可持续的反应介质。通过改变合成温度和溶剂水分数，该方法使用高效、快速（10分钟）微波加热来控制氧化铁相、尺寸和形态。用纯DES合成得到小（
Here, we present a new microwave-solvothermal method for the preparation of iron oxide nanostructures using deep eutectic solvents as a more sustainable reaction medium. By varying the synthesis temperature and solvent water fraction, the methodology offers control over iron oxide phase, size, and morphology, using efficient, rapid (10 minute) microwave heating. Synthesis with pure DES gives small (