Effect of Co‐Precipitation on the Low‐Temperature Sintering of Biphasic Calcium Phosphate
Effect of Co‐Precipitation on the Low‐Temperature Sintering of Biphasic Calcium Phosphate
复制标题
共沉淀对双相磷酸钙低温烧结的影响
DOI:
10.1111/j.1551-2916.2006.00977.x
复制
发表时间:
2006
影响因子:
3.9
通讯作者:
Y. Kong
中科院分区:
文献类型:
--
作者:
Youn;Seong‐Hyeon Hong;Y. Kong
Three types of biphasic calcium phosphate (BCP) powders were prepared and their sintering behavior was investigated. The specific surface area and HA/TCP ratio were similar in all three specimens. Most of the densification in the co-precipitated s-BCP occurred before the β- to α-TCP phase transformation, and a maximum density of ∼95% was obtained at 1100°C. The mixture of separately precipitated and calcined hydroxyapatite (HA) and tricalcium phosphate (TCP) (m-BCP) showed a poor sintering behavior, and the apparent density was below 70% at temperatures up to 1200°C. In the commercial HA and TCP mixture (c-BCP), the low temperature sintering was poor, but densification continued without the phase transformation due to the presence of MgO, achieving almost full densification at 1200°C.