Present status of 920 MHz high-resolution NMR spectrometers
Present status of 920 MHz high-resolution NMR spectrometers
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920 MHz高分辨率核磁共振波谱仪的现状
DOI：
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发表时间：
2004
影响因子：
1.8
通讯作者：
H. Wada
中科院分区：
文献类型：
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作者：
T. Kiyoshi;H. Maeda;J. Kikuchi;Y. Ito;H. Hirota;S. Yokoyama;S. Ito;T. Miki;M. Hamada;O. Ozaki;S. Hayashi;N. Kurihara;H. Suematsu;M. Yoshikawa;S. Matsumoto;A. Sato;H. Wada
第一台920 MHz高分辨率核磁共振(核磁共振)磁体在国立材料科学研究所筑波磁体实验室成功安装。自2002年4月以来，21.6T的持续运行一直没有任何问题。从2002年12月到2003年1月，观测到了0.31赫兹/小时的极好的场稳定性。自2002年7月以来，该磁体被用作世界上唯一的920 MHz高分辨率核磁共振谱仪的重要组成部分。用质子选择探头测量0.1%乙苯的信噪比高达2981。一个HCN三重共振探头现在被连接到光谱仪上，为日本的国家蛋白质结构和功能分析项目做出贡献。第二台920兆赫级核磁共振光谱仪定于2004年春完工。
The first 920 MHz high-resolution NMR (nuclear magnetic resonance) magnet was successfully installed at the Tsukuba Magnet Laboratory of the National Institute for Materials Science. A persistent operation at 21.6 T has continued since April 2002 without any problems. Excellent field stability of 0.31 Hz/h was observed from December 2002 to January 2003. Since July 2002, the magnet was used as an essential part of the only 920 MHz high-resolution NMR spectrometer in the world. The signal-to-noise ratio of 0.1% ethylbenzene using a proton-selective probe was as high as 2981. An HCN triple-resonance probe is now attached to the spectrometer to contribute to the National Project on Protein Structural and Functional Analysis in Japan. The completion of the second 920 MHz-class NMR spectrometer is scheduled for spring 2004.
DOI：
10.1073/pnas.92.20.9279
发表时间：
1995-09-26
影响因子：
11.1
作者：
TOLMAN, JR;FLANAGAN, JM;PRESTEGARD, JH
通讯作者：
PRESTEGARD, JH