Piezoelectric glass-ceramics produced via oriented growth of Sr2TiSi2O8 fresnoite: thermal annealing of surface modified quenched glasses

Piezoelectric glass-ceramics produced via oriented growth of Sr2TiSi2O8 fresnoite: thermal annealing of surface modified quenched glasses
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DOI:
10.1039/c2ce25933h
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发表时间:
2012-01-01
期刊:
影响因子:
3.1
通讯作者:
Ruessel, Christian
Ruessel, Christian
中科院分区:
化学3区
文献类型:
--
作者:
Patschger, Marek;Wisniewski, Wolfgang;Ruessel, Christian

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抛光具有2SrO中心点TiO2中心点2.75 SiO2组成的玻璃样品,随后用石墨或氧化铝粉末覆盖,最后在970 ℃下退火20小时以诱导表面结晶。利用X射线衍射(XRD)和电子背散射衍射(EBSD)分析了表面处理对生长过程中的择优晶向的影响。此外,表面处理对压电d(33)值的影响进行了描述,并参考抛光样品退火没有预先的表面处理。
Glass samples with the composition 2SrO center dot TiO2 center dot 2.75 SiO2 were polished, subsequently covered with graphite or alumina powder and finally annealed at 970 degrees C for 20 h in order to induce surface crystallisation. The effect of the surface treatment on the preferred crystal orientations during growth into the bulk is analyzed using X-ray diffraction (XRD) and electron backscatter diffraction (EBSD). Furthermore, the effect of the surface treatment on the piezoelectric d(33)-value is described and referenced to polished samples annealed without previous surface treatment.