A High-Resolution 43 Ca Solid-State NMR Study of the Calcium Sites of Hydroxyapatite
A High-Resolution 43 Ca Solid-State NMR Study of the Calcium Sites of Hydroxyapatite
复制标题
羟基磷灰石钙位点的高分辨率 43 Ca 固态核磁共振研究
DOI:
10.1021/ja710557t
复制
发表时间:
2008
影响因子:
15
通讯作者:
Laurencin D
中科院分区:
文献类型:
--
作者:
Laurencin D
High resolution43Ca solid-state NMR studies of hydroxyapatite (Ca10(PO4)6(OH)2) were performed at 14.1 T. The two crystallographically distinct calcium sites were unequivocally resolved by a triple-quantum magic angle spinning experiment, and the unambiguous assignment of the signals was possible using1H-43Ca rotational echo double resonance and1H-43Ca cross polarization magic angle spinning experiments.