Improved Synthesis of 1,4,5,8,9,12-Hexaazatriphenylenehexacarboxylic Acid

Improved Synthesis of 1,4,5,8,9,12-Hexaazatriphenylenehexacarboxylic Acid
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1,4,5,8,9,12-六氮杂苯并菲六甲酸的改进合成

DOI:
10.1055/s-1994-25480
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发表时间:
1994
期刊:
Synthesis
影响因子:
--
通讯作者:
A. Czarnik
A. Czarnik
中科院分区:
--
文献类型:
--
作者:
J. Rademacher;K. Kanakarajan;A. Czarnik

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六氮杂苯并菲 (HAT) 衍生物(包括标题化合物)的合成先前已有报道。然而,由于纯度、收率低和溶剂昂贵等问题,它们的潜在用途尚未完全实现。我们现在报告了 HAT 衍生物的改进合成,产量高、纯度高,并且不使用昂贵的溶剂
The synthesis of hexaazatriphenylene (HAT) derivatives, including the title compound, have been reported previously. However, due to problems with purity, low yields and expensive solvents, their potential utility has yet to be fully realized. We now report the improved synthesis of HAT derivatives in good yields, high purity, and without the use of expensive solvents