Microwave-Enhanced High-Speed Fluorous Synthesis.
Microwave-Enhanced High-Speed Fluorous Synthesis.
复制标题
微波增强高速氟合成。
DOI：
10.1007/128_045
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发表时间：
2006
影响因子：
8.6
通讯作者：
Zhang,Wei
中科院分区：
文献类型：
--
作者：
Zhang,Wei
提高反应速度和简化产物纯化是提高有机合成效率的两大途径。提出了微波加热与氟净化相结合的高速固相合成新工艺。综述了微波增强含氟合成的各种技术及其在pd催化交叉偶联反应、自由基反应、多组分反应和化合物库合成等方面的应用。
Increasing reaction speed and simplifying product purification are two major ways to improve the efficiency of organic synthesis. A new technology for high-speed solution-phase synthesis has been developed by combination of microwave heating and fluorous purification. This review describes different techniques for microwave-enhanced fluorous synthesis and their applications in Pd-catalyzed cross-coupling reactions, free-radical reactions, multicomponent reactions, and compound library synthesis.