Synthesis of ZIF-11 crystals by microwave heating
Synthesis of ZIF-11 crystals by microwave heating
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DOI：
10.1039/c9nj04589a
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发表时间：
2020-03
影响因子：
3.3
通讯作者：
Jolie M. Lucero;Taylor J. Self;Moises A. Carreon
中科院分区：
文献类型：
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作者：
Jolie M. Lucero;Taylor J. Self;Moises A. Carreon
我们展示了通过微波辅助方法合成沸石咪唑酯骨架ZIF-11。所得2-7 μm晶体在几分钟内合成，BET表面积高达745 m2 g−1。综述了ZIF-11的合成技术。XRD、SEM和孔隙率测定法作为关键的表征技术。
We demonstrate the synthesis of zeolitic imidazolate framework ZIF-11 via a microwave assisted approach. The resultant 2–7 μm crystals were synthesized in minutes and displayed BET surface areas as high as 745 m2 g−1. The state-of-the-art ZIF-11 synthesis techniques are summarized. XRD, SEM, and porosimetry were used as pivotal characterization techniques.