Advanced Transmission Electron Microscopy: Imaging and Diffraction in Nanoscience by Jian Min Zuo and John C.H. Spence
Advanced Transmission Electron Microscopy: Imaging and Diffraction in Nanoscience by Jian Min Zuo and John C.H. Spence
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DOI:
10.1007/978-1-4939-6607-3
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发表时间:
2016-10
期刊:
影响因子:
5
通讯作者:
J. Zuo;J. Spence
中科院分区:
文献类型:
--
作者:
J. Zuo;J. Spence
This book is written and organized around three topics: electron diffraction, electron optics, and electron crystallography. It is intended as an advanced undergraduateor graduate-level text in support of course materials in materials science, physics, or chemistry departments. High-resolution transmission electron microscope imaging and scanning transmission electron microscopy are treated as major applications of electron optics, as well as powerful electron crystallographic techniques for structure determination. The emphasis here is on the fundamentals and applications of electron diffraction and imaging in materials research, especially in the study of nanoscience. For this purpose, we have included theory for electron wave propagation, electron diffraction and imaging, and a detailed treatment of electron optics, aberration correction, and instrument techniques, on a level that can be followed by a materials science or physics graduate student. For crystallography, we have emphasized the fundamentals of symmetry, structure and bonding, diffuse scattering, imaging of defects, strain measurement, and determination of nanostructures. Structure determination of large crystals, including polymeric and biological samples, is not discussed specifically in this book, although the electron diffraction and imaging theories presented here and instrumental techniques apply equally to these topics.Transmission electron microscopy (TEM) traditionally refers to electron diffraction and imaging techniques that are enabled by a transmission electron microscope (with the same TEM acronym). Scanning transmission electron microscopy (STEM) embodies a separate set of techniques. The development of modern TEMs that function as both TEM and STEM has brought them together, as complementary techniques, often abbreviated as S/TEM. For this reason, we have simply used TEM in the book’s title. STEM, more than TEM, is associated with powerful analytical techniques, such as electron energy loss spectroscopy and energy-dispersive X-ray spectroscopy. This aspect of TEM is not covered here, and readers are referred to the excellent books on these subjects by Egerton (2011), Hawkes and Spence (2007), and Pennycook and Nellist (2011).