Nano-structural observation of in situ silica in natural rubber matrix by three dimensional transmission electron microscopy
Nano-structural observation of in situ silica in natural rubber matrix by three dimensional transmission electron microscopy
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DOI：
10.1002/marc.200400053
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发表时间：
2004-06-21
影响因子：
4.6
通讯作者：
Kohjiya, S
中科院分区：
文献类型：
--
作者：
Ikeda, Y;Katoh, A;Kohjiya, S
首次利用 3D 透射电子断层扫描技术观察到橡胶 (NR) 中颗粒的三维 (3D) 纳米结构。该方法使我们能够以纳米级分辨率可视化和评估 3D 空间中的结构特征，例如通过四乙氧基硅烷的溶胶-凝胶反应在 NR 基质中生成的原位二氧化硅的尺寸和体积。
The three dimansional (3D) nanostructure of particulate in rubber (NR) were observed for the first time by use of 3D transmission electron tomography. The method enabled us to visualize and evaluate structural charachteristics in 3D space, such as the size and the volume of in situ silica generated in the NR matrix by the sol-gel reaction of tetraethoxysilane, at nanometer scale resolution.