Structural studies of alpha-bungarotoxin. 1. Sequence-specific 1H NMR resonance assignments.
Structural studies of alpha-bungarotoxin. 1. Sequence-specific 1H NMR resonance assignments.
复制标题
α-金环蛇毒素的结构研究。
DOI：
10.1021/bi00408a016
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发表时间：
1988
期刊：
影响因子：
2.9
通讯作者：
Kuntz,ID
中科院分区：
文献类型：
--
作者：
Basus,VJ;Billeter,M;Love,RA;Stroud,RM;Kuntz,ID
材料和方法α-银环蛇毒素的分离和纯化描述于本系列的第三篇论文（Kosen等，1988年）。缩写：NMR，核磁共振; 2D，二维; NOE，核奥弗豪泽效应; NOESY，2D NOE光谱; COSY，2D/-相关光谱; HOHAHA，2D Homeland Hartmann-Hahn光谱; HRNOESY，HOHAHA中继相干转移NOE光谱; TSP，钠（三甲基甲硅烷基）-丙酸酯; ppm，百万分率; y，旋磁比; Hu射频场强; tu演化时间; t2，数据采集时间; U1，傅立叶变换的t，维数; a2，傅立叶变换的t2维数。
Materials and MethodsIsolation and purification of a-bungarotoxin is described in the third paper of this series (Kosen et al., 1988). Samples were prepared by dissolving the lyophilized powder in either1 Abbreviations: NMR, nuclear magnetic resonance; 2D, two dimensional; NOE, nuclearOverhauser effect; NOESY, 2D NOE spec-troscopy; COSY, 2D/-correlated spectroscopy; HOHAHA, 2D homonuclear Hartmann-Hahn spectroscopy; HRNOESY, HOHAHA relayed coherence transfer NOE spectroscopy; TSP, sodium (trimethylsilyl)-propionate; ppm, parts per million; y, gyromagnetic ratio; Hu radio frequency field strength; tu evolution time; t2, data acquisition time; u,, Fourier transformed t, dimension; a2, Fourier transformed t2 dimension.