One-step preparation of poly(vinyl alcohol)-protected Pt nanoparticles through a heat-treatment method

One-step preparation of poly(vinyl alcohol)-protected Pt nanoparticles through a heat-treatment method
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DOI:
10.1016/j.matlet.2006.08.047
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发表时间:
2007-04
期刊:
影响因子:
3
通讯作者:
Yonglan Luo;Xuping Sun
Yonglan Luo;Xuping Sun
中科院分区:
材料科学3区
文献类型:
--
作者:
Yonglan Luo;Xuping Sun

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A heat-treatment method for the preparation of well-stable, polymer-protected Pt nanoparticles in the range of 2–7 nm in diameter is demonstrated. The formation of Pt nanoparticles occurs in a single step process, carried out by heating an aqueous solution containing a poly(vinyl alcohol) polymer and H2PtCl6, with the use of PVA to serve as both a reducing reagent and a protective reagent. The Pt nanoparticles were characterized by UV–vis absorption spectra, transmission electron microscopy (TEM), and X-ray photoelectron spectrum (XPS) and the Pt nanoparticle formation process was further investigated by in situ UV–vis experiment.