Applications of solid-phase micro- extraction with mass spectrometryin pesticide analysis
Applications of solid-phase micro- extraction with mass spectrometryin pesticide analysis
复制标题
固相微萃取质谱在农药分析中的应用
DOI：
10.1002/jssc.201800804
复制
发表时间：
2019
影响因子：
3.1
通讯作者：
Liu Huwei
中科院分区：
文献类型：
--
作者：
Liang Dapeng;Liu Wenjie;Raza Rabia;Bai Yu;Liu Huwei
农药在农业生产中的应用十分广泛，其产生的转化产物种类繁多，其持续使用会对生态系统造成危害。高效、灵敏的农药样品富集和分析技术是非常必要的。与其他萃取方法相比，固相微萃取是一种无溶剂、经济、稳定、通用、高通量的样品前处理技术，特别适用于复杂基质中农药的分析。固相微萃取-气相色谱-质谱联用技术和液相色谱-质谱联用技术在农药分析中得到了广泛的应用。另一方面，近年来，固相微萃取快速分离和环境质谱快速检测的结合提供了高效的农药筛选。本文综述了固相微萃取-质谱联用技术在农药分析中的应用。
Pesticides, widely applied in agriculture, can produce a variety of transformation products and their continuous use causes deleterious effects to ecosystem. Efficient and sensitive analytical techniques for enrichment and analysis of pesticides samples are highly required. Compared with other extraction methods, solid‐phase micro extraction is a solvent free, cost effective, robust, versatile, and high throughput sample preparation technique, especially for the analysis of pesticides from complicated matrices. Coupling of solid‐phase micro extraction with gas chromatography and mass spectrometry and liquid chromatography–mass spectrometry has been extensively applied in pesticide analysis. On the other hand, in recent years, combination of fast separation using solid‐phase micro extraction and rapid detection using ambient mass spectrometry is providing highly efficient pesticide screening. This article summarizes the applications of solid‐phase micro extraction coupled to mass spectrometry for pesticides analysis.