INTERFERENCES IN SOLID-PHASE EXTRACTION USING C-18 BONDED POROUS SILICA CARTRIDGES

INTERFERENCES IN SOLID-PHASE EXTRACTION USING C-18 BONDED POROUS SILICA CARTRIDGES
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DOI:
10.1021/ac00164a021
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发表时间:
1988-07-01
影响因子:
7.4
通讯作者:
RICHARD, JJ
RICHARD, JJ
中科院分区:
化学1区
文献类型:
--
作者:
JUNK, GA;AVERY, MJ;RICHARD, JJ

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已对市售固相萃取(SPE)柱的程序空白进行了表征。通过提取柱的组分并通过GC/MS分析这些提取物,将烷烃、烯烃、增塑剂和抗氧化剂鉴别为可能的干扰化合物。在使用SPE柱的程序空白中也观察到提取物中鉴别的大多数化合物。
Procedural blanks from commercial solid-phase extraction (SPE) cartridges have been characterized. Alkanes, alkenes, plasticizers, and antioxidants were identified as possible interference compounds by extracting components of the cartridges and by analyzing these extracts by GC/MS. Most of the compounds identified in the extracts were also observed in the procedural blanks from use of the SPE cartridges.