Synthesis of 6-hydroxy-2-methyl-3-thioxo-2H-1,2,4-triazin-5-one
Synthesis of 6-hydroxy-2-methyl-3-thioxo-2H-1,2,4-triazin-5-one
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DOI：
10.1080/00397919608003566
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发表时间：
1996-01-01
影响因子：
2.1
通讯作者：
Tyler, JW
中科院分区：
文献类型：
--
作者：
Branch, CL;Eggleston, DS;Tyler, JW
以2-甲基氨基硫脲为原料，经酰化、环合、阳离子交换层析三步反应制得标题化合物。它是充分的特点，通常的光谱手段，以及通过N-15核磁共振光谱和X-射线晶体学分析。
The title compound has been prepared in three steps from 2-methylthiosemicarbazide following acylation, cyclisation and cation exchange chromatography. It was fully characterised by the usual spectroscopic means as well as by N-15 nmr spectroscopy and X-ray crystallographic analysis.