Effect of Sintering Temperature and Packing Powder on the Properties of Pb(Zr,Ti,Mg,Zn,Nb)O3 Ceramic

Effect of Sintering Temperature and Packing Powder on the Properties of Pb(Zr,Ti,Mg,Zn,Nb)O3 Ceramic
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烧结温度和填料粉末对Pb(Zr,Ti,Mg,Zn,Nb)O3陶瓷性能的影响

DOI:
10.1143/jjap.42.l595
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发表时间:
2003
影响因子:
1.5
通讯作者:
Chun
Chun
中科院分区:
物理与天体物理4区
文献类型:
--
作者:
Chun

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研究了烧结温度和填充粉对PbO_3陶瓷性能的影响。在1250℃烧结3h时,材料的介电和压电性能达到最大值,过高的烧结温度会导致PbO的大量损失和组成的变化,从而导致显微结构的不均匀和焦绿石相的存在。焦绿石相对介电和压电性能不利。具有优良压电性能的PZT-PMN-PZN(PZT-PMN-PZN)系PZT-PMN-PZN(PZT-PMN-PZN)系PZT-PMN-PZN系具有优良的压电性能,以未烧成的粉末为填充粉提供正蒸汽压。
The effect of sintering temperature and packing powder on the properties of Pb(Zr,Ti,Mg,Zn,Nb)O3 ceramic was studied. Dielectric and piezoelectric properties have maximum values at the sintering temperature of 1250°C for 3 h. A higher sintering temperature causes excessive PbO loss and a resultant variation in composition, which leads to an inhomogeneous microstructure and the emergence existence of a pyrochlore phase. The pyrochlore phase is detrimental to the dielectric and piezoelectric properties. The Pb[(Zr,Ti)0.74(Mg1/3Nb2/3)0.20(Zn1/3Nb2/3)0.06]O3 (PZT-PMN-PZN) piezoceramic system, which has excellent piezoelectric properties, uses uncalcined powder of the main component as the packing powder to provide a positive vapor pressure.