Improved data acquisition in grazing-incidence X-ray scattering experiments using a pixel detector

Improved data acquisition in grazing-incidence X-ray scattering experiments using a pixel detector
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DOI:
10.1107/s0108767305014790
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发表时间:
2005-07-01
影响因子:
1.8
通讯作者:
Eikenberry, EF
Eikenberry, EF
中科院分区:
材料科学3区
文献类型:
--
作者:
Schlepütz, CM;Herger, R;Eikenberry, EF

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在掠入射 X 射线实验中使用区域探测器在速度和可靠性方面具有许多优势。这里讨论了使用瑞士光源开发的皮拉图斯像素探测器建立的程序,用于优化材料科学光束线上表面衍射数据的数据采集和分析,特别是在反射率测量、晶体截断和分数阶棒以及掠入射衍射实验方面。
The use of an area detector in grazing-incidence X-ray experiments lends many advantages in terms of both speed and reliability. Here a discussion is given of the procedures established using the PILATUS pixel detector developed at the Swiss Light Source for optimizing data acquisition and analysis of surface diffraction data at the Materials Science beamline, especially with regard to reflectivity measurements, crystal truncation and fractional order rods, and grazing-incidence diffraction experiments.