Synthesis and magnetic properties of nanocolumnar nickel films deposited in argon-nitrogen atmosphere

Synthesis and magnetic properties of nanocolumnar nickel films deposited in argon-nitrogen atmosphere
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氩氮气氛沉积纳米柱状镍薄膜的合成及磁性能

DOI:
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发表时间:
2012
期刊:
影响因子:
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通讯作者:
V. Burkhovetskii
V. Burkhovetskii
中科院分区:
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文献类型:
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作者:
A. Linnik;A. Prudnikov;R. Shalaev;V. Varyukhin;S. Kostyrya;V. Burkhovetskii

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在氮气体积分数为2%的Ar气氛中,通过磁控溅射镍靶,获得了具有垂直于衬底生长的纳米柱结构的铁磁性镍膜。X射线衍射测量和磁性研究表明,所获得的薄膜由氮在镍中的固溶体组成。薄膜的饱和磁化强度比纯镍的相应值小1.5-2倍,居里温度低30K。薄膜材料表现出尺寸效应:当颗粒尺寸减小到10 nm以下时,磁化强度急剧下降;当颗粒尺寸为0.5 nm时,薄膜没有磁性有序。
Ferromagnetic nickel films with a structure comprising nanocolumns grown perpendicular to a substrate have been obtained by magnetron sputtering of a nickel target in argon atmosphere containing 2 vol % nitrogen. Measurements of X-ray diffraction and investigation of magnetic properties showed that the obtained films consist of a solid solution of nitrogen in nickel. The saturation magnetization of the films is 1.5–2 times smaller and their Curie temperature is 30 K lower than the corresponding values for pure nickel. The film material exhibits a dimensional effect: as the grain size decreases below 10 nm, the magnetization sharply drops; at a grain size of 0.5 nm, the film possesses no magnetic order.