Assessment of olive oil adulteration by reversed-phase high-performance liquid chromatography amperometric detection of tocopherols and tocotrienols

Assessment of olive oil adulteration by reversed-phase high-performance liquid chromatography amperometric detection of tocopherols and tocotrienols
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DOI:
10.1007/bf02577844
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发表时间:
1995-12-01
影响因子:
2
通讯作者:
Tagliaferri, E
Tagliaferri, E
中科院分区:
农林科学4区
文献类型:
--
作者:
Dionisi, F;Prodolliet, J;Tagliaferri, E

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A method involving reversed-phase high-performance liquid chromatography with amperometric detection has been developed for the analysis of tocopherols and tocotrienols in vegetable oils. The sample preparation avoids saponification. Recoveries of a-tocotrienol and gamma-tocotrienol in extra virgin olive oil were 97.0 and 102.0%, respectively. No tocotrienols were detected in olive, hazelnut, sunflower, and soybean oils, whether virgin or refined. However, relatively high levels of tocotrienols were found in palm and grapeseed oils. This method could detect small quantities (1-2%) of palm and grapeseed oils in olive oil or in any tocotrienol-free vegetable oil and might, therefore, help assess authenticity of vegetable oils.