Molten salt synthesis of SnS2 microplate particles
Molten salt synthesis of SnS2 microplate particles
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DOI：
10.1016/j.matlet.2009.01.010
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发表时间：
2009-04
影响因子：
3
通讯作者：
Hui Xiao;Y. Zhang;Haixin Bai
中科院分区：
文献类型：
--
作者：
Hui Xiao;Y. Zhang;Haixin Bai
介绍了一种熔盐法合成SnS2纳米板的方法，在250-280℃空气中二氯化锡和硫脲的熔体中反应0-5h，然后用蒸馏水洗涤。X射线衍射、拉曼光谱和场发射扫描电子显微镜图像表明，所得产物均为晶相纯的六方SnS2纳米片，厚度为20-70 nm。
A molten salt method to synthesize SnS2nanoplates, in a melt of tin dichloride and thiourea in air at 250–280 °C for 0–5 h, coupled with a subsequent washing treatment using distilled water, is demonstrated. The X-ray diffraction, Raman spectra, and field emission scanning electron microscope images disclosed that all the obtained products were phase pure hexagonal SnS2nanoplates, of 20–70 nm thickness.