Measurement of magnetic susceptibility and calculation of shape factor of NMR samples

Measurement of magnetic susceptibility and calculation of shape factor of NMR samples
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DOI:
10.1016/j.jmr.2005.09.009
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发表时间:
2006-02-01
影响因子:
2.2
通讯作者:
Hoffman, RE
Hoffman, RE
中科院分区:
化学3区
文献类型:
--
作者:
Hoffman, RE

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本文介绍了一种精确测量AIL核磁共振管磁化率和形状因子的方法。将精确的形状系数测定与磁化率测量相结合,可提高化学位移测量的准确度。这对于比较不同溶剂或不同条件下的样品非常重要,例如温度、溶剂和pH。(C)2005 Elsevier Inc.保留所有权利。
A method for accurate measurement of magnetic susceptibility and determination of the shape factor in ail NMR tube is shown. The combination of accurate shape factor determination with susceptibility measurement leads to improved accuracy when measuring chemical shift. This is important for comparing samples in different solvents or under different conditions, such as temperature, solvent, and pH. (c) 2005 Elsevier Inc. All rights reserved.