Basic evaluation on physical properties of experimental fluorinated soft lining materials
Basic evaluation on physical properties of experimental fluorinated soft lining materials
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DOI：
10.4012/dmj.2010-084
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发表时间：
2011-01-01
影响因子：
2.5
通讯作者：
Hishimoto, Munemitsu
中科院分区：
文献类型：
--
作者：
Kasuga, Yuta;Takahashi, Hidekazu;Hishimoto, Munemitsu
本研究的目的是比较含氟单体的软衬材料与传统材料的临床应用所需的性能，以开发具有长期稳定粘弹性的新型软衬材料。对四种软衬材料进行了检测。制备了含有甲基丙烯酸十二氯庚酯（SR 12 F）和甲基丙烯酸十三氯辛酯（SR 13 F）的两种实验材料。两个商业软衬材料，一个丙烯酸基和一个硅橡胶基，被选为参考材料。评价了海岸A硬度、粘弹性能、吸水性、溶解性和耐沾污性。海岸A硬度和位移用双因素方差分析（ANOVA）和Tukey's HSD检验进行分析。采用单因素方差分析和Tukey's HSD检验分析了吸水性、溶解性和颜色变化。显著性水平设定为0.05。与商业产品相比，SR12F和SR13F显示出更大的粘性流动、低吸水性、低溶解度和良好的耐沾污性。结果表明，含氟单体的软衬材料可能具有潜在的长期稳定的粘弹性行为。
The purpose of the present study was to compare the properties required for the clinical application of soft lining materials containing a fluorinated monomer versus that of conventional materials in an effort to develop a new soft lining material with long-term stable viscoelastic properties. Four soft lining materials were examined. Two experimental materials containing dodecafluoroheptyl methacrylate (SR12F) or tridecafluorooctyl methacrylate (SR13F) were prepared. Two commercial soft lining materials, one acrylic-based and one silicone rubber-based, were selected as reference materials. Shore A hardness, viscoelastic properties, water sorption, solubility, and staining resistance were evaluated. The Shore A hardness and the displacements were analyzed with two-way analysis of variance (ANOVA) and Tukey's HSD test. The water sorption, the solubility and the color change were analyzed with one-way ANOVA and Tukey's HSD test. The significance level was set at 0.05. SR12F and SR13F showed greater viscous flow, low water sorption, low solubility, and good staining resistance compared to the commercial products. The results indicate that the soft lining materials containing fluorinated monomers might have a potentially long-term stable viscoelastic behavior.