A modular microreactor for mixed acid nitration
A modular microreactor for mixed acid nitration
复制标题
DOI：
10.1002/ceat.200500096
复制
发表时间：
2005-07-01
影响因子：
2.1
通讯作者：
Winterbauer, H
中科院分区：
文献类型：
--
作者：
Henke, L;Winterbauer, H
研制了一种由聚四氟乙烯和钽制成的耐腐蚀微反应器，用于模拟不同的硝化反应。由于模块化的结构类型，新的微反应器可以很容易地适应工业工厂的条件，并且在大多数情况下，结果可以直接按比例放大，不需要中试规模的工厂。新的微反应器可用于等温以及绝热硝化，和热不稳定和敏感的化合物可以生产的整个反应器可以在非常低的温度下操作。
A corrosion resistant microreactor made of PTFE and Tantalum has been developed for the simulation of different nitration reactions. The new microreactor can be easily adapted to the conditions in an industrial plant due to the modular type of construction, and in most cases the results can be directly scaled up and pilot scale plants are not required. The new microreactor can be used for isothermal as well as for adiabatic nitrations, and thermally unstable and sensitive compounds can be produced as the whole reactor can be operated at very low temperatures.