Benchtop flow-NMR for rapid online monitoring of RAFT and free radical polymerisation in batch and continuous reactors
Benchtop flow-NMR for rapid online monitoring of RAFT and free radical polymerisation in batch and continuous reactors
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DOI：
10.1039/c9py00982e
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发表时间：
2019-09-21
影响因子：
4.6
通讯作者：
Warren, Nicholas J.
中科院分区：
文献类型：
--
作者：
Knox, Stephen T.;Parkinson, Sam;Warren, Nicholas J.
“台式”NMR光谱仪用于离线和实时详细监测在间歇和连续反应器中进行的受控和自由基聚合。这使得详细的动力学分析与前所未有的时间分辨率的反应，达到在五分钟内接近完成。
A "Benchtop" NMR spectrometer is used for detailed monitoring of controlled and free radical polymerisations performed in batch and continuous reactors both offline and in real-time. This allows detailed kinetic analysis with unprecedented temporal resolution for reactions which reach near completion in under five minutes.