In-situ SEM and TEM tensile observations of novel Co-Al-W-Mo-Ta-B-Ce alloys with a coherent γ-CoSS/γ’-Co3(Al,W) microstructure at room temperature

In-situ SEM and TEM tensile observations of novel Co-Al-W-Mo-Ta-B-Ce alloys with a coherent γ-CoSS/γ’-Co3(Al,W) microstructure at room temperature
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室温下具有相干 γ-CoSS/γ-Co3(Al,W) 微观结构的新型 Co-Al-W-Mo-Ta-B-Ce 合金的原位 SEM 和 TEM 拉伸观察

DOI:
10.1016/j.msea.2017.04.040
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发表时间:
2017-06
期刊:
Materials Science & Engineering A
影响因子:
--
通讯作者:
J. B. Sha
J. B. Sha
中科院分区:
其他
文献类型:
--
作者:
F. Zhong;Y. Y. Xin;S. S. Li;J. B. Sha

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利用SEM和TEM原位研究了γ ′-Co 3(Al,W)强化的Co-9Al-4.5W-4.5Mo-2 Ta-0.02B-(0.01,0.1)Ce合金(以下分别称为0.01Ce合金和0.1Ce合金)的滑移带-晶界相互作用。对于具有γ/γ ′-Co 3(Al,W)共格组织的0.01Ce合金,{111}<1 1 0>位错在γ通道中萌生,随后切入相邻的γ ′相。小角度晶界(LAGB)是必要的滑移带转移机制。当引入易滑移系的对齐因子M&gt;0.8和引出滑移系的Schmid因子&gt;0.3时,滑移带通过LAGB转移。大角度晶界(HAGB)通常具有低M值,并且传入的滑移带在HAGB处被阻挡而不转移;相反,邻近晶粒中具有最高Schmid因子的独立滑移系统被激活。γ/γ ′-Co 3(Al,W)组织的塑性变形和滑移带-晶界的相互作用使0.01Ce合金的伸长率达到16.4%。在0.1Ce合金的晶界处有一些Co 3 W沉淀物,滑移带绕过、切穿或有时被沉淀物阻止,导致2.1%的低延伸率和混合的韧窝和解理失效。
Slip band-grain boundary interactions of γ’-Co3(Al,W)-strengthened Co-9Al-4.5W-4.5Mo-2Ta-0.02B-(0.01, 0.1)Ce alloys (referred to as 0.01Ce alloy and 0.1Ce alloy, respectively, hereafter) were investigated in-situ using SEM and TEM. For the 0.01Ce alloy with a γ/γ’-Co3(Al, W) coherent microstructure, the {1 1 1}<1 1 0> dislocations initiate in the γ channels and subsequently cut into the neighbouring γ’ phase. A low-angle grain boundary (LAGB) is necessary for the slip band transfer mechanism. The slip bands transfer through the LAGB when the alignment factor M>0.8 with the incoming easy-slip system and the Schmid factor >0.3 on the outgoing slip system. The high-angle grain boundaries (HAGBs) usually have a low M value and the incoming slip bands are blocked at the HAGBs without transfer; instead, independent slip systems with the highest Schmid factor in the neighbouring grain are activated. The plastic deformation of the γ/γ’-Co3(Al,W) microstructure and the slip band-grain boundary interactions lead to an elongation of 16.4% of the 0.01Ce alloy. With some Co3W precipitates at the grain boundary of the 0.1Ce alloy, the slip bands bypass, cut through, or sometimes are arrested by the precipitates, resulting in a low elongation of 2.1% and a mixed dimple and cleavage failure.
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