Preparation of Bi2S3 nanorods by microwave irradiation
Preparation of Bi2S3 nanorods by microwave irradiation
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DOI：
10.1016/s0025-5408(01)00734-6
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发表时间：
2001-11-01
影响因子：
5.4
通讯作者：
Chen, HY
中科院分区：
文献类型：
--
作者：
Liao, XH;Wang, H;Chen, HY
Bi2S3纳米棒，直径约。 10 nm，长度可达约。 300 nm，已通过微波辐射从硝酸铋和硫脲的甲醛溶液中成功制备。粉末X射线衍射(XRD)图表明产物为纯斜方Bi2S3相。该产品还通过透射电子显微镜（TEM）和X射线光电子能谱（XPS）技术进行了表征。 (C) 2001 Elsevier Science Ltd. 保留所有权利。
Bi2S3 nanorods, with a diameter of ca. 10 nm and a length of up to ca. 300 nm, have been successfully prepared from a formaldehyde solution of bismuth nitrate and thiourea by microwave irradiation. Powder X-ray diffraction (XRD) pattern indicates that the product is pure orthorhombic Bi2S3 phase. The product is also characterized by the techniques of transmission electron microscopy (TEM) and X-ray photoelectron spectra (XPS). (C) 2001 Elsevier Science Ltd. All rights reserved.