(E)-3-Bromo-N'-(5-bromo-2-hydroxy-benzyl-idene)benzohydrazide.

(E)-3-Bromo-N'-(5-bromo-2-hydroxy-benzyl-idene)benzohydrazide.
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(E)-3-溴-N-(5-溴-2-羟基-亚苄基)苯甲酰肼。

DOI:
10.1107/s1600536808030675
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发表时间:
2008
期刊:
Acta crystallographica. Section E, Structure reports online
影响因子:
--
通讯作者:
Wang,Xiao-Ya
Wang,Xiao-Ya
中科院分区:
--
文献类型:
--
作者:
Qu,Lan-Zhu;Yang,Tao;Cao,Guo-Biao;Wang,Xiao-Ya

文献摘要

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标题化合物C14H10Br2N2O2是由5-溴水杨醛与等摩尔量的3-溴苯甲酰肼在甲醇中反应合成的。两个苯环之间的二面角为10.5 (4)°。在晶体结构中,分子间通过N-H⋯O氢键连接形成平行于c轴的链,分子内还发生O-H⋯N相互作用。
The title compound, C14H10Br2N2O2, was synthesized by the reaction of 5-bromosalicylaldehyde with an equimolar quantity of 3-bromobenzohydrazide in methanol. The dihedral angle between the two benzene rings is 10.5 (4)°. In the crystal structure, molecules are linked through intermolecular N—H⋯O hydrogen bonds to form chains parallel to the c axis, and an intramolecular O—H⋯N interaction also occurs.