A Novel Dual Air-Bearing Fixed-x Diffractometer for Small-Molecule Single-Crystal X-ray Diffraction on Beamline I19 at Diamond Light Source

A Novel Dual Air-Bearing Fixed-x Diffractometer for Small-Molecule Single-Crystal X-ray Diffraction on Beamline I19 at Diamond Light Source
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DOI:
10.3390/cryst7110336
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发表时间:
2017-11-01
期刊:
影响因子:
2.7
通讯作者:
Wooley, Ron W.
Wooley, Ron W.
中科院分区:
材料科学3区
文献类型:
--
作者:
Allan, David R.;Nowell, Harriott;Wooley, Ron W.

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在此,我们描述了一种新型的用于钻石光源光束线I19的双气浮固定衍射仪的研制。衍射仪旨在通过Dectris Pilatus 2M像素阵列光子计数检测器进行快速数据收集,同时允许远程操作与机器人换样器相结合。通过在omega轴和(原文如此)轴上都使用空气轴承,使混乱的球体尽可能小。详细描述了新仪器的设计和构造,并附上了Johnson等人的一篇论文。(也在本期中)将提供用户对其运作的看法。
Herein, we describe the development of a novel dual air-bearing fixed-diffractometer for beamline I19 at Diamond Light Source. The diffractometer is designed to facilitate the rapid data collections possible with a Dectris Pilatus 2M pixel-array photon-counting detector, while allowing remote operation in conjunction with a robotic sample changer. The sphere-of-confusion is made as small as practicably possible, through the use of air-bearings for both the omega and (sic) axes. The design and construction of the new instrument is described in detail and an accompanying paper by Johnson et al. (also in this issue) will provide a user perspective of its operation.