The formation of Mo precipitates in a supersaturated Mo5SiB2 intermetallic phase

The formation of Mo precipitates in a supersaturated Mo5SiB2 intermetallic phase
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DOI:
10.1080/095008399177192
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发表时间:
1999-06
影响因子:
1.2
通讯作者:
R. Sakidja;H. Sieber;J. Perepezko
R. Sakidja;H. Sieber;J. Perepezko
中科院分区:
材料科学4区
文献类型:
--
作者:
R. Sakidja;H. Sieber;J. Perepezko

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Mo70B20Si10合金在铸态1600℃退火后,在有序的Mo5SiB2 (T2)金属间相(D8l)内形成了Mo固溶体(Moss)的板状析出物。通过透射电子显微镜-选择区域电子衍射研究确定了T2基体内Moss片状沉淀的晶体取向,主要显示了{111}Mo (001)T2与Moss T2的关系。高分辨率透射电镜分析表明,经过1600℃2 150 h的长时间退火处理后,仍保持片状形貌,Moss-T2长界面保持半相干。
Upon annealing a Mo70B20Si10 alloy in the as-cast condition at 1600oC, plate shaped precipitates of a Mo solid solution (Moss) have been observed to develop within an ordered Mo5SiB2 (T2) intermetallic phase (D8l). The crystallographic orientation of Moss plate-like precipitates within the T2 matrix has been determined by transmission electron microscopy-selected area electron diffraction studies to show mainly the relations {111} Mo (001)T2 and Moss T2. Upon a prolonged annealing treatment at 1600oC for2 150 h, the plate-like morphology was still maintained and the Moss-T2 long interface remained semicoherent as confirmed by high-resolution transmission electron microscopy analysis.