Magic-Angle-Spinning NMR Magnet Development: Field Analysis and Prototypes.
Magic-Angle-Spinning NMR Magnet Development: Field Analysis and Prototypes.
复制标题
魔角旋转核磁共振磁体开发:现场分析和原型。
DOI:
10.1109/tasc.2013.2245934
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发表时间:
2013
期刊:
影响因子:
--
通讯作者:
Iwasa,Yukikazu
中科院分区:
文献类型:
--
作者:
Voccio,John;Hahn,Seungyong;Park,DongKeun;Ling,Jiayin;Kim,Youngjae;Bascuñán,Juan;Iwasa,Yukikazu
We are currently working on a program to complete a 1.5 T/75 mm RT bore magic-angle-spinning nuclear magnetic resonance magnet. The magic-angle-spinning magnet comprises az-axis 0.866-T solenoid and anx-axis 1.225-T dipole, each to be wound with NbTi wire and operated at 4.2 K in persistent mode. A combination of the fields creates a 1.5-T field pointed at 54.74 degrees (magic angle) from the rotation (z) axis. In the first year of this 3-year program, we have completed magnetic analysis and design of both coils. Also, using a winding machine of our own design and fabrication, we have wound several prototype dipole coils with NbTi wire. As part of this development, we have repeatedly made successful persistent NbTi-NbTi joints with this multifilamentary NbTi wire.