Sealed rotors for in situ high temperature high pressure MAS NMR.
Sealed rotors for in situ high temperature high pressure MAS NMR.
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DOI:
10.1039/c5cc03910j
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发表时间:
2015-09-11
期刊:
影响因子:
--
通讯作者:
Lercher JA
中科院分区:
文献类型:
--
作者:
Hu JZ;Hu MY;Zhao Z;Xu S;Vjunov A;Shi H;Camaioni DM;Peden CH;Lercher JA
Here we present the design of reusable and perfectly-sealed all-zircornia MAS rotors. The rotors are used to study AlPO4-5 molecular sieve crystallization under hydrothermal conditions, high temperature high pressure cyclohexanol dehydration reaction, and low temperature metabolomics of intact biological tissue.