Formation of monolithic silica gel microhoneycombs (SMHs) using pseudosteady state growth of microstructural ice crystals

Formation of monolithic silica gel microhoneycombs (SMHs) using pseudosteady state growth of microstructural ice crystals
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DOI:
10.1039/b316597c
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发表时间:
2004-04-07
影响因子:
4.9
通讯作者:
Tamon, H
Tamon, H
中科院分区:
化学2区
文献类型:
--
作者:
Mukai, SR;Nishihara, H;Tamon, H

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整体式硅胶微蜂窝的结构中有一排直立的大孔,其壁上有发达的微孔/介孔,它是通过冰晶的准稳态生长制备的,这种生长发生在新鲜凝胶的水凝胶的单向冻结-凝胶化过程中,然后是一种保护孔隙的干燥方法,即冷冻干燥。
Monolithic silica gel microhoneycombs, which have an array of straight macropores within their structure and developed micro/mesopores inside their walls, were prepared using pseudosteady state growth of ice crystals which occurs during the unidirectional freeze-gelation of freshly gelled aqueous silica hydrogels, followed by a pore-protecting drying method, freeze drying.