Complete assignments of 1H and 13C NMR spectral data of nine surfactin isomers
Complete assignments of 1H and 13C NMR spectral data of nine surfactin isomers
复制标题
DOI:
10.1002/mrc.2048
复制
发表时间:
2007-09-01
影响因子:
2
通讯作者:
Yao, Xin-Sheng
中科院分区:
文献类型:
--
作者:
Tang, Jin-Shan;Gao, Hao;Yao, Xin-Sheng
A new surf actin isomer (1) was isolated from a mangrove bacteria strain 'Bacillus sp'. Its structure was identified, and full assignments of H-1 and C-13 NMR spectral data were achieved for the first time by a combination of mass spectrometry and 1D and 2D NMR experiments including DEPT, H-1-H-1 COSY, HSQC, HMBC, TOCSY, ROESY, and HSQC-TOCSY. The NMR spectral data of eight known analogs (2-9) are also reported. Copyright (C) 2007 John Wiley & Sons, Ltd.