Oxidation of thiols to disulfides with molecular bromine on hydrated silica gel support
Oxidation of thiols to disulfides with molecular bromine on hydrated silica gel support
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DOI：
10.1016/s0040-4039(02)01220-0
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发表时间：
2002-08-26
影响因子：
1.8
通讯作者：
McDermott, M
中科院分区：
文献类型：
--
作者：
Ali, MH;McDermott, M
报道了在硅胶固体载体上用分子溴氧化硫醇为二硫化物的结果。该方法利用有机介质，并且不需要碱来中和HBr副产物以抑制酸促进的副反应。硅胶载体的使用简化了后处理和产物分离。(C)2002爱思唯尔科技有限公司。保留所有权利。
Results of oxidation of thiols to disulfides with molecular bromine on silica gel solid support are reported. The procedure utilizes organic media and does not require a base to neutralize HBr by-products to suppress acid promoted side reactions. Utilization of silica gel support simplifies work up and product isolation. (C) 2002 Elsevier Science Ltd. All rights reserved.