Application of inductively coupled plasma mass spectrometry to the simultaneous determination of chlorine, bromine and iodine in the National Bureau of Standards Standard Reference Material 1648 Urban Particulate

Application of inductively coupled plasma mass spectrometry to the simultaneous determination of chlorine, bromine and iodine in the National Bureau of Standards Standard Reference Material 1648 Urban Particulate
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DOI:
10.1039/ja9880300659
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发表时间:
1988
影响因子:
3.4
通讯作者:
A. R. Date;M. Stuart
A. R. Date;M. Stuart
中科院分区:
化学2区
文献类型:
--
作者:
A. R. Date;M. Stuart

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介绍了电感耦合等离子体质谱(ICP-MS)同时测定国家标准局(NBS)1648城市颗粒物标准参考物质(SRM)中氯、溴和碘的方法。说明了ICP-MS在常规溶解程序后同时进行多元素痕量测定的潜力。包括卤化物的各种可能的方法被认为是,和各种样品溶解程序进行了研究。国家统计局SRM 1648城市颗粒物的数据被认为是在以前公布的结果和多原子离子干扰样品融合程序。结果表明,该方法对环境粉尘及其它样品中总氯、溴、碘的测定具有很大的潜力。
The application of inductively coupled plasma mass spectrometry (ICP-MS) to the simultaneous determination of chlorine, bromine and iodine in the National Bureau of Standards (NBS) Standard Reference Material (SRM) 1648 Urban Particulate is described. The potential of ICP-MS for simultaneous multi-element trace determinations after a conventional dissolution procedure is illustrated. Various possible methods for including the halides are considered, and various sample dissolution procedures are investigated. Data presented for the NBS SRM 1648 Urban Particulate are considered in terms of the previously published results and polyatomic ion interferences from sample fusion procedures. It has been shown that the method has great potential for the determination of total chlorine, bromine and iodine in environmental dust and other samples.