Thermogravimetry/Differential Thermal Analysis and Phase Identification of Cs2O·Al2O3·2TiO2 in the Ternary System Cs2O‐A12O3‐TiO2

Thermogravimetry/Differential Thermal Analysis and Phase Identification of Cs2O·Al2O3·2TiO2 in the Ternary System Cs2O‐A12O3‐TiO2
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三元体系Cs2O-A12O3-TiO2中Cs2O·Al2O3·2TiO2的热重/差热分析及物相鉴定

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发表时间:
2006
期刊:
影响因子:
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通讯作者:
C. Freiburg
C. Freiburg
中科院分区:
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文献类型:
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作者:
A. G. Solomah;R. Odoj;C. Freiburg

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对2CsNO_3 + Al_2 O_3 + 2 TiO_2混合物在1530 K以下进行了热重和差热分析。结果表明,合成的产物为正交晶系的Cs2 Al 2 Ti 2 O 8,晶格参数aO=0.996,b 0 =0.898,Co=0.573 nm。同时进行TG/DTA以量化铯的重量损失和挥发,并监测作为温度的函数的相的发展和/或稳定性。
Thermogravimetry and differential thermal analyses were conducted on the mixture 2CsNO3+A12O3+2TiO2 up to 1530 K. The resultant phase was identified as orthorhombic Cs2Al2Ti2O8 with lattice parameters aO=0.996, b0=0.898, and co=0.573 nm. Simultaneous TG/DTA was performed to quantify weight loss and volatilization of cesium and to monitor the development and/or stability of the phase as a function of temperature.