Coordination Polymer Route to Wurtzite ZnS and CdS Nanorods

Coordination Polymer Route to Wurtzite ZnS and CdS Nanorods
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DOI:
10.1006/jssc.2002.9556
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发表时间:
2002-06
影响因子:
5.4
通讯作者:
Zhengping Qiao;Gang Xie;J. Tao;Zhao-Yang Nie;Yan-Zhi Lin;Xiao‐Ming Chen
Zhengping Qiao;Gang Xie;J. Tao;Zhao-Yang Nie;Yan-Zhi Lin;Xiao‐Ming Chen
中科院分区:
工程技术1区
文献类型:
--
作者:
Zhengping Qiao;Gang Xie;J. Tao;Zhao-Yang Nie;Yan-Zhi Lin;Xiao‐Ming Chen

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摘要 以配位聚合物[ M (tp)(4,4′-bipy)] ∞ 在140 ℃溶剂热条件下(M = Zn,Cd)合成了纤锌矿MS纳米棒。通过 TEM 测定的形貌给出了 ZnS 和 CdS 的平均宽度/长度直径分别为 50/200 nm 和 20/75 nm。 X射线粉末衍射和XPS谱证明所制备的产物分别为纯ZnS和CdS。
Abstract Wurtzite MS nanorods were synthesized from coordination polymer [ M (tp)(4,4′-bipy)] ∞ at 140°C under solvothermal condition ( M =Zn, Cd). The morphology determined by TEM gives the average diameters of width/length as 50/200 nm and 20/75 nm for ZnS and CdS, respectively. X-ray powder diffraction and XPS spectra proved that the as-prepared products were pure ZnS and CdS, respectively.