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Hochauflösendes Massenspektrometer

Hochauflösendes Massenspektrometer
高分辨率质谱仪
批准号:
275347340
负责人:
金额:
$0.0万
依托单位国家:
德国
项目类别:
Major Research Instrumentation
财政年份:
2015
资助国家:
德国
项目状态:
未结题
起止时间:
2014-12-31 至 --

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中文摘要
翻译
在无机化学研究所,将安装一台具有多种电离方法的高分辨率质谱仪(ES I, HPLC-ESI, APCI, ASAP, LIDFI),以满足目前活跃的八个研究小组的不同分析要求。在过去的4-5年里,研究所的研究重点显著扩大,任命了5名新教员和两个初级研究小组,导致工作人员(博士生、博士后和长期研究人员)从大约70人增加到120多人,因此迫切需要扩大分析设施。目前,内部可用的质谱分析仅限于GC/MS,这与许多研究人员对温和电离方法(如电喷雾或现场解吸)的要求不匹配。此外,这些单位质量分辨率的单四极杆仪器不允许确定精确的质量和分配和公式。其他安装在学院其他地方的质谱仪已被各自的所有者占用,因此不能共享使用。因此,迫切需要扩大无机化学研究所的质谱设备,以满足依赖多种电离方法的研究人员数量显著增加的分析需求。
英文摘要
At the Institute for lnorganic Chemistry, a high-resolution mass spectrometer with a wide range of ionisation methods (ES I, HPLC-ESI, APCI, ASAP, LIDFI) is to be installed to satisfy the diverse analytical requirements of the eight research groups now active. An expansion of the analytical facilities is urgently needed as the research focus of the institute has significantly broadened within the last 4-5 years with the appointment of five new faculty members and two junior research groups, leading to a concomitant increase in staff members (doctoral students, postdocs, and permanent research staff) from about 70 to over 120. Currently, mass spectrometric analysis available in-house is limited to GC/MS, which does not match the requirements of many researchers for mild ionisation methods such as electrospray or field desorption. Furthermore, these Singlequadrupole instruments with unit mass resolution do not allow determination of exact masses and assignment of sum formulas. Other mass spectrometers installed elsewhere in the faculty are fully occupied by their respective owners and thus not available for shared use. Therefore, the expansion of the mass spectrometric facilities at the Institute for lnorganic Chemistry is urgently required to serve the analytical needs of a significantly increased number of researchers which rely on a diverse spectrum of ionisation methods.
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