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Formulation of Liquid-Liquid-Liquid Reaction System in Microreactor

Formulation of Liquid-Liquid-Liquid Reaction System in Microreactor
微反应器中液-液-液反应体系的制定
批准号:
24656483
负责人:
KUSAKABE Katsuki
金额:
$2.5万
依托单位:
依托单位国家:
日本
项目类别:
Grant-in-Aid for Challenging Exploratory Research
财政年份:
2012
资助国家:
日本
项目状态:
已结题
起止时间:
2012 至 --

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英文摘要
When potassium hydroxide solution, benzene and dichloromethane including equimolar mixture of benzyltriphenylphosphonium bromide and p-methoxybenzaldehyde was fed through a cross joint into a microreactor, segmented flow consisting water droplet and oil droplets was formed and the Wittig reaction proceeded in the tube. The reaction yield in liquid-liquid-liquid reaction system was higher than that in liquid-liquid one due to the contribution of mass transfer effect.
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