Demonstration of the fast track process development and of the optimal operation of the reductive amination of long-chained aldehydes in emulsion systems (D02*)

示范乳液系统中长链醛还原胺化的快速工艺开发和优化操作 (D02*)

• 批准号: 398048376
• 金额: --
• 依托单位: Fachgebiet Dynamik und Betrieb technischer Anlagen
• 依托单位国家: 德国
• 项目类别: CRC/Transregios
• 财政年份: 2018
• 资助国家: 德国
• 起止时间: 2017-12-31 至 2020-12-31
• 项目状态: 已结题
• 来源: https://gepris.dfg.de/gepris/projekt/398048376?language=en
• 关键词: Demonstration; fast; track; process; development

Subproject D2 N comprises a proof of concept and validation of the reductive amination of Undeca-nal in microemulsions in a continuously operated miniplant. The operability of the reaction, the phase separation, and the implementation of a membrane process for water separation are key aspects. Additionally, the plant set-up and relevant analytics will be updated accordingly. To support the fast process development, adaptive optimal experimental design is developed and applied on individual unit operations within the miniplant. Finally, an optimal process design (D1 N) is implemented and optimally operated (D4 N).

子项目D2 N包括在连续操作的小型装置中对十一烷醛在微乳液中的还原胺化进行概念验证和验证。反应的可操作性、相分离和水分离的膜过程的实施是关键方面。此外，工厂设置和相关分析将相应更新。为了支持快速的过程开发，自适应优化实验设计的开发和应用在微型工厂内的单个单元操作。最后，实施最佳工艺设计（D1 N）并最佳地操作（D4 N）。