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超声辅助对激光熔化沉积高温钛合金组织性能的影响机制研究

批准号:
52105356
项目类别:
青年科学基金项目(C类)
资助金额:
30.0 万元
负责人:
刘征
依托单位:
学科分类:
成形制造
结题年份:
2024
批准年份:
2021
项目状态:
已结题
项目参与者:
刘征

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中文摘要
激光熔化沉积(LMD)成形钛合金构件中的冶金缺陷、较大的残余应力和粗大的显微组织是影响构件质量的关键问题,超声辅助LMD技术是优化其成形构件质量的重要方法。目前,针对超声辅助如何影响LMD成形合金构件中冶金缺陷、残余应力和显微组织尚缺乏深入研究。本项目拟以超声辅助LMD成形的Ti60合金作为研究对象,通过CCD、红外相机和同步辐射X射线衍射技术获得不同工艺条件下激光熔池的瞬时形貌、温度分布和熔体流动状态,研究超声诱发的空化和声流效应对激光熔池热力学和动力学行为的影响机制。采用Micro-CT、XRD、TEM、APT、拉伸和原位拉伸等实验系统研究不同工艺参数对超声辅助LMD成形合金中冶金缺陷、残余应力、显微组织和力学性能的影响,结合激光的熔池行为和其凝固特征,揭示超声辅助抑制合金冶金缺陷、弱化合金残余应力、细化合金显微组织的机理,从而为超声辅助LMD成形合金构件质量的优化提供理论依据。
英文摘要
Laser Melt Deposition (LMD), which deposits powder feedstock through a nozzle and melts it with a laser, is one of highly versatile and flexible Additive Manufacturing technologies, enabling layer-by-layer fabrication of complex near-net-shape components. However, rapid solidification during the LMD process causes several technical challenges including the creation of defects, residual stress and coarse epitaxial grains, which act as a barrier to widespread implementation of LMD technique in safety-critical components. To overcome these limitations, a high-energy ultrasonic vibration-assisted (UV-A) process is added in the LMD. Previous studies have shown that the introduction of a high-energy ultrasonic vibration into the melt can result in two nonlinear effects of acoustic streaming and acoustic cavitation, enabling a significant effect on defects and microstructural features of LMD-produced parts. At present, the mechanism of UV-A method in LMD process is still not well understood. Ti60 alloy is a near-α titanium alloy designed for use as high pressure compressors due to its excellent comprehensive performance at elevated temperatures. In this study, Ti60 alloy is fabricated by UV-A LMD under different process conditions. The transient morphology, temperature field and melt flow behavior of the laser molten pool under different process conditions are obtained by CCD, infrared camera and synchronous X-ray diffraction technique, thereby understanding the influence mechanisms of acoustic streaming and acoustic cavitation on the thermodynamic and kinetic behaviors of the laser molten pool. Several experiments, including Micro-CT, XRD, EBSD, TEM, APT, tensile and in-situ tensile etc., are employed to investigate the characteristics of defects, residual stress, microstructure and mechanical properties of the alloy built by UV-A LMD under different process conditions, so that building the relationship between the process parameters and these characteristics. Based on the laser molten pool behaviors and its solidification characteristics, the mechanisms of refining the grain, mitigating the porosity and residual stress via UV-A method in the LMD process are discussed and unraveled, which can provide a theoretical basis for improving mechanical properties of UV-A LDM-produced components, and promote practical application of UV-A LDM-produced titanium alloys.
在激光熔化沉积(LMD)制备过程中引入超声辅助工艺是降低其制备合金冶金缺陷、优化合金组织性能的重要方法,但目前超声辅助对LMD成形高温钛合金中的冶金缺陷、显微组织及力学性能的影响机制尚不明确。本项目以超声辅助LMD成形的Ti60合金为研究对象,系统研究了超声辅助对LMD成形高温钛合金熔池形貌、冶金缺陷、显微组织、晶体学织构及合金力学性能的影响规律,结合模拟仿真深入探讨了超声辅助LMD激光熔池行为和其凝固特征。宏观上,超声振动会显著影响合金的熔池形貌,随着超声频率的增加,激光熔池尺寸及热影响区增大。合金中的孔隙率及孔隙缺陷尺寸会随着超声振动的引入而显著降低。微观上,超声辅助引入的空化效应和声流效应显著改变了合金的微观组织特征,合金内部的粗大初始β柱状晶粒被破碎,等轴晶粒占比增加。随着超声频率的增加,合金的晶粒尺寸先减小后略有增加,但均远低于无超声的样品。当频率为28.5KHz时样品的平均晶粒尺寸最小,直径为151.2μm。此外,超声辅助的引入显著降低了合金中α相片层的长径比、织构强度和位错密度,合金中析出的硅化物的也更加的细小弥散,分布更为均匀。在力学性能方面,施加超声辅助后高温钛合金的横向/纵向(HD/VD)室温及高温拉伸的强度和塑性均得到提升,降低了各向异性。28.5KHz的样品的提升效果最为显著,在HD方向的抗拉强度为1192MPa,断裂伸长率为7.3%,在VD方向的抗拉强度为1174MPa,断裂伸长率为12.1%。两个方向在650℃高温拉伸的强度分别为702MPa和700MPa,断裂延伸率可达40%和57%,均优于无超声样品。在此基础上,进一步研究了合金的变形损伤行为,讨论了超声辅助在抑制合金冶金缺陷及细化合金组织过程中的作用机理,建立合金的制备工艺、显微组织和力学性能三者的量化关系,为进一步调控超声辅助LMD的制备工艺,优化合金力学性能及其一致性提供理论依据。
超声辅助激光增材制造Ti-Al-Si低组元钛合金的素化设计与组织调控及强韧化机理
  • 批准号:
    52565042
  • 项目类别:
    地区科学基金项目
  • 资助金额:
    32.00万元
  • 批准年份:
    2025
  • 负责人:
    刘征
  • 依托单位:
国内基金
海外基金