ANALYSIS OF ETHYL CARBAMATE IN ALCOHOLIC BEVERAGES
ANALYSIS OF ETHYL CARBAMATE IN ALCOHOLIC BEVERAGES
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DOI：
10.1007/bf01027176
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发表时间：
1988-01-01
期刊：
影响因子：
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通讯作者：
LISBJERG, S
中科院分区：
文献类型：
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作者：
FUNCH, F;LISBJERG, S
本文介绍了酒精饮料中氨基甲酸乙酯的分析方法。用气相色谱/质谱仪(GC/MS)系统监测选定的离子进行定量。以重氢氨基甲酸乙酯为内标。本文还介绍了该化合物的合成方法。结果表明，重复性分析偏差较小，回收率接近100%。对几类酒精饮料进行了分析。在每个类别中，都发现了一些超过加拿大限量的样品。该方法只适用于酒精饮料，但经过修改后，它应该适用于任何类型的食品样本。
The paper describes a method for analysing ethyl carbamate in alcoholic beverages. A gas chromatographic/mass spectrometric (GC/MS)-system monitoring selected ions is used for quantification. Deuterated ethyl carbamate is used as the internal standard. The synthesis of this compound is also described. The results show a small deviation on repeated analysis and a recovery of nearly 100%. Several categories of alcoholic beverages were analysed. In each category some samples exceeding the Canadian limits were found. The method is based only on alcoholic beverages, but with modifications it should be applicable to any kind of food sample.